Texture, Stress, and Microstructure
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Statistical Analysis of Misorientation Distributions From Growth Selection
Experiments in Iron–3% Si
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The frequency of occurrence of differently misoriented grain boundaries in growth
selection experiments in silicon–iron was reported by Ibe and Lücke and has been the
basis of many texture models. However, this pattern of behaviour bears much similarity
to misorientation frequencies calculated from random textures. A comparison of the
experimental and computed frequency distribution shows that there are statistically
significant differences and therefore that some possibilities for growth selection do exist (Source: Texture, Stress, and Microstructure)
Source: Texture, Stress, and Microstructure - November 3, 2009 Category: Materials Science Source Type: journals
Microstructure and Texture of in Situ Heavily Drawn Cu–Nb Composites
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Heavily cold drawn in situ Cu–Nb composites have been investigated by transmission
electron microscopy (TEM) and X-ray analysis. Dislocation density in the copper matrix
has been shown to change only slightly in the investigated drawing ratio range because of
the development of stage IV of deformation. In Nb filaments dislocation density in the
investigated range at first increases with deformation and then drops at the highest
drawing ratio. At intermediate deformation niobium grains consist of fine blocks
separated by low-angle dislocation boundaries. At drawing, fibre texture develops in
both phases, with 〈...
Source: Texture, Stress, and Microstructure - November 3, 2009 Category: Materials Science Source Type: journals
Influence of Rolling
Temperature on the Perfection
Degree of Recrystallization
Cube Texture in Nickel
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The effect of the rolling temperature on the deformation texture and the perfection
degree of a cube texture in pure-nickel thin tape were investigated. The kinetics of
primary recrystallization was studied on samples that had undergone rolling at different
temperatures and the temperature of the onset of secondary recrystallization was
determined. Regularities of the structure formation in the samples are discussed. It is
established that the cube texture with the maximum sharpness is produced in the samples
rolled at room temperature. (Source: Texture, Stress, and Microstructure)
Source: Texture, Stress, and Microstructure - November 3, 2009 Category: Materials Science Source Type: journals
Effect of Zonal Isolation on the Kinetics of Sintering a
Particulate Body
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This paper describes the so-called meso-scale simulations of sintering a particulate body.
Computations were made using 3D structure-imitation computer model of evolution of
a powder compact during sintering. It was demonstrated, that in powder bodies the
effect of zonal isolation (forming separate groups of particles during sintering) determines
features of shrinkage and internal structure of a compact. In case of the diffusion-
viscous flow of particles the fact was proved that the zonal isolation is
predetermined by ratio of viscosity and free surface energy. It was verified, that there
is a critical value of the above ...
Source: Texture, Stress, and Microstructure - November 3, 2009 Category: Materials Science Source Type: journals
Quantification of Minor Texture Components by Hard X-Rays
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Non-destructive methods to determine the volume fraction of minor texture components
with very low reflection intensities are presented. The methods are based on polycrystalline
diffraction of hard X-rays from synchrotron sources. By focusing the X-rays and
scanning the specimen, it is shown that volume fractions as low as 10-9 can be registered,
provided that the crystallographic orientations of such volume elements are far away
from any major texture component. Simultaneously, the spatial resolving power is of
the order 0.03 μm3. The relevance of such methods for nucleation studies and trace
analysis is outlined. (...
Source: Texture, Stress, and Microstructure - November 3, 2009 Category: Materials Science Source Type: journals
Recrystallization in a Hot Deformed Al-Mg-Si Alloy: The Effect of Fine Precipitates
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The recrystallization of an Al-Mg-Si alloy deformed by plane strain compression at
400°C and 1 s-1 has been studied. Fine particles are found to have a significant influence
on the development of recrystallization textures. Annealing at 400°C, in the
presence of Al-Fe-Si particles located on boundaries, results in a weak recrystallization
texture. There is a clear indication that grain nucleation is associated with
abnormal subgrain growth. The occurrence of this recovery process is analyzed by
taking into account the particle pinning pressure and the orientation dependence of
boundary energy and mobility. The cu...
Source: Texture, Stress, and Microstructure - November 3, 2009 Category: Materials Science Source Type: journals
Microtexture Studies of PST and PZT Ceramics and PZT Thin Film by Electron Backscatter Diffraction Patterns
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Crystallographic orientations of twelve different lead scandium tantalate (PST) ceramics,
two lead zirconate titanate ceramics (PZT) and one PZT thin film were investigated by
the technique of electron backscatter diffraction (EBSD) in the scanning electron microscope.
The PST ceramics were processed under different conditions of temperature and
annealing. Crystal orientations in the bulk ceramics were examined and the results were
plotted in microtexture pole- and inverse pole-figures. Local texture and misorientation
between adjacent grains in certain selected regions of the ceramics were also examined.
To compare the re...
Source: Texture, Stress, and Microstructure - November 3, 2009 Category: Materials Science Source Type: journals
On The Peculiarities of X-Ray Determination of Crystallographic Texture in Samples After Testing Wear Resistance
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A peculiar relief generally appears on the sample surface while testing wear resistance,
which impairs the results of texture analysis by X-ray diffraction methods. The main
reason for this is screening influence of the surface roughness on the X-ray passing
through. From model representations, the influence on the screening of the relief
parameters and the characteristic angle of reflection of X-rays is shown. Distribution
of the parameters of a relief that actually forms is analyzed. A computer-assisted
method of calculation of pole figures that excludes the screening effect is suggested.
As an example of the method of a...
Source: Texture, Stress, and Microstructure - November 3, 2009 Category: Materials Science Source Type: journals
Effective Elastic Properties of Textured Cubic Polycrystals
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A general scheme for the solution of problem of averaging elastic properties of textured polycrystals is suggested which is based on the algebraic methods of description of elastic properties. (Source: Texture, Stress, and Microstructure)
Source: Texture, Stress, and Microstructure - November 3, 2009 Category: Materials Science Source Type: journals
Pole Figure Inversion Using Finite Elements Over Rodrigues Space
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Using finite elements over Rodrigues space, methods are developed for the formation
and inversion of pole figures. The methods take advantage of the properties of
Rodrigues space, particularly the fact that geodesics corresponding to pole figure projection
paths are straight lines. Both discrete and continuous pole figure data may be
inverted to obtain orientation distribution functions (ODFs) in Rodrigues space, and
we include sample applications for both types of data. (Source: Texture, Stress, and Microstructure)
Source: Texture, Stress, and Microstructure - November 3, 2009 Category: Materials Science Source Type: journals
Preface
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(Source: Texture, Stress, and Microstructure)
Source: Texture, Stress, and Microstructure - November 3, 2009 Category: Materials Science Source Type: journals
Depth Resolved Strain and Phase Mapping of Dissimilar Friction Stir Welds Using High Energy Synchrotron Radiation
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The strain and phase distribution in a dissimilar friction stir weld of AA6082-T6 to AA2024-T3 is investigated
non-destructively. The measurements are performed using a novel depth resolved strain and phase mapping
technique. The technique is based on the use of a focussed high energy synchrotron beam, a novel spiral slit
system, and an area detector system. Through thickness measurements of the residual strain along the weld
centre show strong variations with changes of sign. The strain scans across the weld exhibit a strong asymmetry
in particular for the longitudinal strain component. A depth resolved strain mapping acr...
Source: Texture, Stress, and Microstructure - November 3, 2009 Category: Materials Science Source Type: journals
Tensile Deformation Induced Texture Transformation in Austenitic Stainless Steel
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Texture patterns of the starting ώ and transformed α structural phases were obtained from AISI 304 stainless
steel sheets subjected to varying levels of tensile deformation using high energy X-ray diffraction in combination
with the texture enhanced Rietveld method. The use of this method allows the simultaneous determination
of the orientation distribution functions (ODF) of both phases, even for small α-martensite fractions of
the order of 5%. The texture patterns are analyzed in terms of the crystallographic orientation relation
between the starting and transformed phases and the preferential form...
Source: Texture, Stress, and Microstructure - November 3, 2009 Category: Materials Science Source Type: journals
Torsion Texture Measurements With High-Energy Synchrotron Radiation on NiAl
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Diffraction with high-energy synchrotron radiation is a new experimental method to determine textures of
materials, which due to the special properties of this radiation, in the future may have advantages in terms
of accuracy of local texture measurements in comparison to established methods like Electron back scatter
diffraction (EBSD). In the present study NiAl polycrystals with two different initial textures have been
deformed in torsion at 727°C and 1000°C and their texture development has been measured with highenergy
synchrotron radiation. Torsion enables the study of texture formation with strain as well a...
Source: Texture, Stress, and Microstructure - November 3, 2009 Category: Materials Science Source Type: journals
Full Stress Tensor Determination in A textured Aerospace Aluminium Alloy Plate Using synchrotron X-Ray Diffraction
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Triaxial strain scanning has been performed on a 7mm thick 7150-aluminium alloy Variable Polarity Plasma
Arc (VPPA) weld using synchrotron X-rays. It has been demonstrated that the use of specific advantageous
(hkl) peaks that occur in this highly textured aerospace alloy plate permits fast deep measurements in reflection
as well as in transmission. The sin2ψ method was also utilised to monitor the variation in deviatoric stress
component (σ11−σ33) across the weld in both the test-piece and a comb like reference specimen used to map the
changes in stress-free lattice spacings over the we...
Source: Texture, Stress, and Microstructure - November 3, 2009 Category: Materials Science Source Type: journals
Use of Synchrotron Diffraction Data for Describing Crystal Structure and Crystallographic Phase Analysis of R-Phase NiTi Shape Memory Alloy
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The objective of the present article is to use the third generation synchrotron X-ray source at the
European Synchrotron Research Facility (ESRF) in Grenoble, which make available X-ray beams of
higher energy and much higher intensity than laboratory X-ray sources, for describing crystal structure of
the R-phase in 50.75 at.% Ti–47.75 at.% Ni–1.50 at.% Fe ternary alloy. The synchrotron diffraction data
of R-phase were analyzed using the Rietveld refinement with GSH description. The results showed that no
significant improvement in fit is found when the inversion center is removed from the P3¯ mode...
Source: Texture, Stress, and Microstructure - November 3, 2009 Category: Materials Science Source Type: journals
Influence of Grain Number on Graphite Quantitative Texture Study
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The present work is devoted to the study of the grain number influence on the quantitative texture analysis
and on the values of averaged elastic properties. Number of grains does not influence mathematical definition
of orientation distribution function (ODF) (Bunge, H.J. (1982). Texture Analysis in Material Science.
Butterworths, London; Matthies, S., Vinel, G.W. and Helming, K. (1987). Standard Distributions in
Texture Analysis. Akademie-Verlag, Berlin.); nevertheless, intuitively clear that, averaging procedure implies
a ‘‘large’’ number of grains to make sense. In the present work we applied the already sugges...
Source: Texture, Stress, and Microstructure - November 3, 2009 Category: Materials Science Source Type: journals
Applications on High-Energy X-Rays to Stress Measurements of Thermal Barrier Coatings
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High-energy X-rays from a synchrotron radiation source, SPring-8, were applied to the stress measurements
of thermal barrier coating (TBC). The specimen had a zirconia top coat on a bond coat of NiCoCrAlY
sprayed on the substrate of Ni-base super alloys. The stress in the bond coat was measured through the
top coat using the diffraction of Ni3Al 311 by high-energy X-rays with an energy of 72 keV. The sin2ψ method was used to determine the stress value. A specially designed furnace with a wide beryllium window
was developed to conduct in-situ measurements of the internal stress in the bond coating at the room tempera...
Source: Texture, Stress, and Microstructure - November 3, 2009 Category: Materials Science Source Type: journals
High-Energy X-Rays: A tool for Advanced Bulk Investigations in Materials Science and Physics
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The combination of these techniques is a strong issue for the construction and development of future
instruments. (Source: Texture, Stress, and Microstructure)
Source: Texture, Stress, and Microstructure - November 3, 2009 Category: Materials Science Source Type: journals
High-Resolution Imaging of Texture and Microstructure by the Moving Detector Method
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In order to describe texture and microstructure of a polycrystalline material completely, crystal orientation
g={ϕ1Φϕ2} must be known in all points x={x1 x2 x3} of the material. This can be achieved by locationresolved
diffraction of high-energy, i.e. short-wave, X-rays from synchrotron sources. Highest resolution in
the orientation- as well as the location-coordinates can be achieved by three variants of a detector “sweeping”
technique in which an area detector is continuously moved during exposure. This technique results in
two-dimensionally continuous images which are sec...
Source: Texture, Stress, and Microstructure - November 3, 2009 Category: Materials Science Source Type: journals
Hot-Extruded and Cold-Rolled Textures of the Matrix Aluminum in Deformation Processed Two-Phase Nb/Al Metal-Metal Composites
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In this article, the powder metallurgy technique combined with flat hot-extrusion and cold rolling processes
was employed to fabricate 10 and 20vol.%Nb/Al metal–metal composite sheets. The hot-extruded and coldrolled
textures of the matrix aluminum in these metal–metal composite sheets were investigated by three
dimensional orientation distribution functions (ODFs) analysis. The results show that the extrusion mode
and large second phase particulate metal, Nb, have strong influence on the development of the extrusion
and cold rolling textures in composites’ matrix. The matrix Al forms β-fiber textures afte...
Source: Texture, Stress, and Microstructure - November 3, 2009 Category: Materials Science Source Type: journals
Intensity Correction in Texture Measurement of Polycrystalline Thin Films by X-Ray Diffraction
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The tilting of a specimen may not only result in defocusing effect, but also in a change of irradiated volume
during texture measurement for thin films and coatings by using X-ray diffraction. The influence on diffraction
intensity has to be considered in order to obtain an accurate result of texture analysis. The effect of irradiated
volume can be formulated as a function of the thickness and the linear absorption of a studied film
material, the tilt angle of the specimen and the Bragg angle of diffraction, and then eliminated. In view of
that the preparation of a randomly oriented specimen would be difficult, a simple an...
Source: Texture, Stress, and Microstructure - November 3, 2009 Category: Materials Science Source Type: journals
Effect of Gravity on the Kinetics of Consolidation of Powder Bodies
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Physical mathematical model of sintering powders is suggested with respect to the influence of gravitation on
sintering kinetics. Structure genesis and evolution in sintered glass-based particulate bodies is investigated
both in computer simulations and “in situ”. (Source: Texture, Stress, and Microstructure)
Source: Texture, Stress, and Microstructure - November 3, 2009 Category: Materials Science Source Type: journals
Using Individual Spectra Simulation for the Study of Pole Figures Errors
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Crystallographic texture is described by pole figures. In this paper, we continue to study experimental pole figure errors. In other words it can be named pole figure measurement errors. These errors are connected with the experimental procedure and do not depend on any further computations. In our previous works it was shown that the qualitative behaviour of pole figure measurement errors is similar to peak width determination errors. To check this conclusion a set of diffraction spectra were measured for Mg + 4.5%Al + 1%Zn sample on the spectrometer for quantitative texture analysis (SKAT) at FLNP, JINR, Dubna. T...
Source: Texture, Stress, and Microstructure - July 8, 2009 Category: Materials Science Source Type: journals
The Texture of a Slate From Nantlle, Caernarvon, North Wales
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A specimen of Cambrian slate from the slate belt in North Wales has been thinned by the ion bombardment
technique to produce an ultrathin section with the specimen plane normal to the cleavage plane. This specimen
has been investigated with the electron microscope by electron transmission. Selected area diffraction patterns allow
identification of individual sheet silicate grains. The pole figures of the basal planes of two sheet silicate minerals,
muscovite and chlorite, have been measured with an X-ray pole-figure goniometer and both show an elongated
maximum normal to the slaty cleavage, with orthorhombic symmetry. Whil...
Source: Texture, Stress, and Microstructure - June 30, 2009 Category: Materials Science Source Type: journals
The Spherical Sample Method in Neutron Diffraction Texture Determination
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Neutron diffraction proves advantageous as compared to X-ray diffraction in texture analysis because of the lower
absorption coefficient for a broad variety of materials especially metals. The spherical sample method is recommended
because it yields the most reliable results and it does not require great preparational efforts. The fundamental
difference between the spherical sample method in X-ray and in neutron diffraction is discussed. (Source: Texture, Stress, and Microstructure)
Source: Texture, Stress, and Microstructure - June 30, 2009 Category: Materials Science Source Type: journals
Texture of Metals
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A condensed review of casting, deformation, and annealing textures of polycrystalline metals and alloys is presented. It is intended to provide an informative but simplified reference for researchers, engineers, and students who are seeking quick information on the development of textures in various metal objects, and for those who are primarily interested in the textures of non-metallic materials, but wish to acquire a general background knowledge on the texture formation in metals. (Source: Texture, Stress, and Microstructure)
Source: Texture, Stress, and Microstructure - June 30, 2009 Category: Materials Science Source Type: journals
Texture Control and the Yield Anisotropy of Plane Strain Magnesium Extrusions
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The textures developed in magnesium, annealed after both hot and cold extrusion under essentially plane strain
conditions, have been qualitatively accounted for in terms of the operative deformation modes. It is found that the
main features of both textures are explained by the operation of {101¯2} and {101¯1} twinning together with basal slip,
but there is an important component of the hot extrusion annealing texture not found in the cold extrusions
texture which can only be explained by the action of {101¯0} or {101¯1} slip. (Source: Texture, Stress, and Microstructure)
Source: Texture, Stress, and Microstructure - June 30, 2009 Category: Materials Science Source Type: journals
X-Ray Analysis of a Quartz Fabric From the Sambagawa Crystalline Schist, Japan
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An X-ray fabric analysis of quartz grains from the Sambagawa crystalline schist, Japan, whose c-axis fabric
(optically measured) was regarded as corresponding to an ultimate steady-state pattern of preferred orientation
of c-axes developed by the approximately non-rotational two-dimensional strain under the Sambagawa metamorphicconditions,
has been made by a texture goniometer for reflection. It has been clarified that [0001] and [101¯]
directions are preferably oriented in the plane of the longest and shortest principal axes of the strain ellipsoid of
mean strain of the system concerned and at the angles of ca. 35...
Source: Texture, Stress, and Microstructure - June 30, 2009 Category: Materials Science Source Type: journals
Anisotropy in Some Soft Magnetic Materials
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Orientation distribution data are presented for low carbon steel and silicon iron after different rolling and
annealing schedules. Magnetic properties which depend solely on orientation can be well described using such
distributions. A general analysis is demonstrated by which other properties may be divided into two components
which are respectively dependent and independent of orientation. An example of this, a.c. power loss, is considered
in detail. It is shown that the orientation-dependence of power loss derives entirely from the hysteresis component.
The classical eddy current loss together with an ‘anomalous&...
Source: Texture, Stress, and Microstructure - June 30, 2009 Category: Materials Science Source Type: journals
The Development of Rolling Textures in Low-Carbon Steels
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The crystallite orientation distribution analysis was applied to the study of the development of the rolling textures
in low-carbon steels. It was found that the constraining effect of the grain boundary remarkably influences the
rolling textures of polycrystalline iron. This enhances the crystal rotations, which would not be expected to occur
in single crystals; and grains having the {110}〈112〉 orientations are forced to rotate about the 〈111〉axes lying
in the sheet normal direction toward the {110}〈110〉 orientations. This is the origin of the 〈111〉
fiber textur...
Source: Texture, Stress, and Microstructure - June 30, 2009 Category: Materials Science Source Type: journals
Topographic Arrangement of Crystallite Orientations in Rolled Copper
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In single and polycrystalline copper rolled to a reduction of 95 %, the topographic arrangements of crystallite
orientations were determined over large areas by means of electron microscopy. Correlated data on orientation,
diffraction site, and transmission pictures in three cross-sections perpendicular to the normal, rolling and transverse
directions were obtained and evaluated. These results were complemented by X-ray studies of the texture. The
rolled polycrystalline structure consists of roughly disc-shaped regions of uniform orientation which are fairly
strongly misoriented with respect to each other. The planes ...
Source: Texture, Stress, and Microstructure - June 30, 2009 Category: Materials Science Source Type: journals
A System of FORTRAN for Three-Dimensional Texture Analysis
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A system of FORTRAN programmes is being described which allows most of the standard problems of three-dimensional texture analysis to be easily carried out. It requires about 25 K memory space and it may easily be enlarged by incorporating further subroutines. (Source: Texture, Stress, and Microstructure)
Source: Texture, Stress, and Microstructure - June 30, 2009 Category: Materials Science Source Type: journals
Texture Development in Ferritic Stainless Steel Sheet
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Two grades of ferritic stainless steels (495 and 410.types) containing about 13 % chromium have been processed by
cold rolling with intermediate and final anneals. The development of textures has been followed and the plastic
anisotropy of the annealed sheet has been assessed. Processing conditions for the development of anisotropy
favourable for deep drawing applications have been defined for the 405 type stainless steel. The evolution of the
favourable {554} 〈225〉 texture component appears to be progressive throughout the processing. It is particularly
well-developed after two moderate cold rolling re...
Source: Texture, Stress, and Microstructure - June 30, 2009 Category: Materials Science Source Type: journals
The Development of the Rolling Texture of Iron Determined by Neutron-Diffraction
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The development of the rolling texture of a low carbon steel was investigated by neutron diffraction calculating three-dimensional orientation distribution functions. The textures consist of two limited fibre axis components A and B centered about (1¯1¯1)[1¯21]+5∘
and (001)[1¯10] respectively with an angle of rotation of about 70∘. For rolling degrees larger than 50% the intensity of the fibre axis component A is being modulated so as to favour the orientation (1¯1¯2)[1¯10]. The texture may be considered as inverse to the low concentration brass texture i...
Source: Texture, Stress, and Microstructure - June 30, 2009 Category: Materials Science Source Type: journals
Oriented Nucleation in Low-Carbon Steels
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The preferred orientations in hot-rolled, cold-rolled (70 % reduction), and annealed low-carbon steels (capped and aluminium-killed grades) have been investigated. Particular attention has been paid to the factors that control texture formation during annealing. (Source: Texture, Stress, and Microstructure)
Source: Texture, Stress, and Microstructure - June 30, 2009 Category: Materials Science Source Type: journals
Automatic Drawing of Stereographic Nets
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The present paper describes a computer program for the automatic tracing of new stereographic nets aimed at the description of pole figures. (Source: Texture, Stress, and Microstructure)
Source: Texture, Stress, and Microstructure - June 30, 2009 Category: Materials Science Source Type: journals
Earing in Deep-Drawing Steels
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The variations of the fourth-order coefficients of the crystallite orientation distribution function, with rolling reduction have been determined after cold-rolling and annealing for a deep-drawing quality rimming steel and an aluminium-killed steel. These coefficients influence drawability and earing behaviour and by the manipulation of
the coefficients in the distribution function of a 60% cold-rolled and annealed rimming steel, a hypothetical non-earing sheet texture has been derived. By comparison with the actual sheet texture those textural components which most affect earing behaviour are identified. (Source: Te...
Source: Texture, Stress, and Microstructure - June 30, 2009 Category: Materials Science Source Type: journals
Cyclic Textures in Aluminium Wires
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Three-dimensional orientation distribution functions were calculated from neutron diffraction pole figures of unwound
cylinders taken at different distances from the centre of cold drawn Al-wires. Their features change from
the axially symmetric type at the very centre of the wire towards a texture near to the rolling type at the surface.
Relations between the three-dimensional function and ordinary fibre texture pole figures were used to study the
dependence of the textures on certain processing variables for cold drawn as well as recrystallized wires. (Source: Texture, Stress, and Microstructure)
Source: Texture, Stress, and Microstructure - June 30, 2009 Category: Materials Science Source Type: journals
Comments on the Determination of Wire Textures
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(Source: Texture, Stress, and Microstructure)
Source: Texture, Stress, and Microstructure - June 30, 2009 Category: Materials Science Source Type: journals
Description of Orientation Distributions of Cubic Crystals by Means of 3-D Rotation Coordinates
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A method has been described to represent orientations and orientation distributions of cubic crystals by means of
a 3-dimensional orientation space which is formed by the repeatedly discussed rotation coordinates (axis and
angle of rotation). Special emphasis has been given to the problem of multi-valency of the representation due to
the cubic symmetry, to the description of scattering around an ideal orientation and to the numerical evaluation
of these orientation coordinates by means of rotation matrices. (Source: Texture, Stress, and Microstructure)
Source: Texture, Stress, and Microstructure - June 30, 2009 Category: Materials Science Source Type: journals
A Test of the Refinement Procedure for
Determining the Crystallite Orientation
Distribution: Polyethylene Terephthalate
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A test of the refinement procedure for improving the crystallite orientation distribution function is presented for a
fiber texture sample of polyethylene terephthalate. This is a particularly difficult example because the triclinic unit
cell offers no simplification due to symmetry, and the pole figures are sharply peaked. The analysis employed 17
observed pole figures and an additional 29 unobserved pole figures reconstructed from the crystallite orientation
distribution function. After three cycles of refinement, in which the maximum value of the coefficient was increased
from 6 to 16, the standard deviations, σq...
Source: Texture, Stress, and Microstructure - June 30, 2009 Category: Materials Science Source Type: journals
The Nucleation of Recrystallisation and the Development of Textures in Heavily Compressed Iron-Carbon Alloys
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Quantitative studies of textures developed in compressed iron–0.02%C and iron–0.14%C alloys before and after annealing have allowed theoretical predictions based on homogeneous plasticity theory to be assessed. It is concluded that qualitatively the theory is very good but predicts rates of texture development rather higher than those observed. The prediction of the theory that orientations on a line joining [110] and [411] should have a tendency to split into two components on deformation and form transition bands, which may be important in nucleating recrystallisation, has been confirmed by the re...
Source: Texture, Stress, and Microstructure - June 30, 2009 Category: Materials Science Source Type: journals
Authors' Reply to Comments on the Determination of Wire Textures
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(Source: Texture, Stress, and Microstructure)
Source: Texture, Stress, and Microstructure - June 30, 2009 Category: Materials Science Source Type: journals
Using Individual Spectra Simulation for the Study of Pole Figures Errors
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Crystallographic texture is described by pole figures. In this paper, we continue to study experimental pole figure errors. In other words it can be named pole figure measurement errors. These errors are connected with the experimental procedure and do not depend on any further computations. In our previous works it was shown that the qualitative behaviour of pole figure measurement errors is similar to peak width determination errors. To check this conclusion a set of diffraction spectra were measured for Mg + 4.5%Al + 1%Zn sample on the spectrometer for quantitative texture analysis (SKAT) at FLNP, JINR, Dubna. T...
Source: Texture, Stress, and Microstructure - June 25, 2009 Category: Materials Science Source Type: journals
Texture and Grain Size Control During Annealing of an Al-SiC Composite Material
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The effects of different heat treatments on the recrystallized texture and grain
size of 90% cold rolled aluminium reinforced by 2vol% SiC whiskers have been studied.
Annealing temperatures in the range 250-510°C and 3 heating rates (25, 80, 400°C/min)
were used. The recrystallization textures were determined by neutron diffraction and
the grain sizes were measured by optical microscopy. It was found that the recrystallization
textures are rotated cube textures ({100} <013 >) and the strength depends
strongly on annealing temperature, (T) and heating rat...
Source: Texture, Stress, and Microstructure - June 10, 2009 Category: Materials Science Source Type: journals
Defocusing in the Reflexion Technique for the Determination of Preferred Orientation Using EDXRD
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The defocusing effect in the reflexion technique for the determination of the preferred orientation using energy-dispersive x-ray diffraction (EDXRD) method is studied experimentally. The measurements show that the defocusing effect is dependent on the Bragg angle, the receiving slit width, the reflexion hkl and the metallurgical condition of the specimen. The defocusing correction or at least the optimizing of the measuring geometry is found to be necessary in quantitative texture measurements. (Source: Texture, Stress, and Microstructure)
Source: Texture, Stress, and Microstructure - June 10, 2009 Category: Materials Science Source Type: journals
Quantitative Determination of Preferred Orientation by Energy-Dispersive X-Ray Diffraction
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The use of energy-dispersive X-ray diffraction
for quantitative determination of preferred
orientations in polycrystalline specimens is analysed.
The method is applied to determinations of
rolling texture and fibre texture. The adaptability
of the method to in situ studies is demonstrated by
observations of texture changes simultaneous with
the deformation of a specimen in a tension test. (Source: Texture, Stress, and Microstructure)
Source: Texture, Stress, and Microstructure - June 10, 2009 Category: Materials Science Source Type: journals
Effect of Crystal Rotation on Earing in Cup Drawing of Highly Textured Materials
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In this paper, a numerical model taking into account of crystal rotation is presented to predict earing
in cup drawing. The model is based on the Continuum Mechanics of Textured Polycrystals and the
assumption of plane strain. Ear profiles have been predicted for some common crystallographic
orientations in face-centered cubic metals and highly textured sheets. It was shown that the major trends
of the predicted profiles for both the single crystals and highly textured sheets were consistent with
experimental results. The effect of crystal rotation on earing was shown to be insignificant for the
predicted ear profiles. How...
Source: Texture, Stress, and Microstructure - June 10, 2009 Category: Materials Science Source Type: journals
Texture Investigations by Neutron Time-of-Flight Diffraction
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For the majority of isotopes the thermal neutron absorption cross section is two or
more orders lower than that for X-rays. This makes neutron diffraction well-suited
for bulk texture investigations. Some characteristics of neutron diffraction are
discussed. The principles of neutron time-of-flight diffraction are described. The pole
figure determination by means of TOF technique is considered. The main parameters
of the present Dubna texture facility are given. Further developments of the
experimental technique are considered. The application of the TOF technique for
inverse pole figure measurement is discussed as an appr...
Source: Texture, Stress, and Microstructure - June 10, 2009 Category: Materials Science Source Type: journals
